Phase Characterization of TiO2 Powder by XRD and TEM
Keywords:
TiO2, anatase, rutile, micro and nanopowders, TEM, XRDAbstract
In this study, the commercial TiO2 nanopowder and micropowder of anatase phase and rutile phase have been characterized by x-ray diffraction (XRD) and transmission electron microscopy (TEM). XRD patterns of nano-TiO2 in rutile and anatase phases exhibit broad peaks whereas both phases of micro-TiO2 demonstrate very sharp peaks. TEM images show that the grain size of TiO2 micropowders and TiO2 nanopowders are 0.3-0.7 μm and 10 nm, respectively. The selected-area electron diffraction patterns of TiO2 nanopowders in rutile and anatase phases are consistent with XRD results.
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online 2452-316X print 2468-1458/Copyright © 2022. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/),
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